Composition #1: Romussi, Giovanni., Ciarallo, Giovanni., Falsone, Gioacchino., Schneider, Claudia. Constituents of Boraginaceae. Triterpene saponins from Anchusa officinalis. liebigs annalen der chemie, 1979, vol. (12), p. 2028–35. .
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Plant part:
Aerial part of plants (as part-nature) (A166F)
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Extraction/Preparation method:
Solvent extraction (A0BZR)
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Additional extraction description:
Ethanol
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Substance:
pentacyclic triterpene saponins (RF-00004334-PAR)
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Additional substance description:
Anchuchosides 1, 2 and 7
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Analytical method code:
Standard Chromatographic tests (paper- thin layer- and column chromatography) (F016A)
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Analytical method - additional description:
IR, ‘H-NMR and MS measurements
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Yes/No Qualitative:
Positive/Present (POS)
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Result type:
Qualitative Value (Binary) (BIN)
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Internal remarks:
Anchusosides ( pentacyclic triterpene saponins)
Composition #2: Huizing, H. J., De Boer, F., Hendriks, H., Balraadjsing, W., Bruins, A. P. Positive and negative ion chemical ionization mass spectrometry of trimethylsilyl derivatives of pyrrolizidine alkaloids using amine radical and hydroxide as the reactant ions. biomedical & environmental mass spectrometry, 1986, vol. 13, no. 6, p. 293–8. .
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Plant part:
Unspecified (A07XD)
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Extraction/Preparation method:
Solvent extraction (A0BZR)
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Additional extraction description:
unspecified
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Substance:
Pyrrolizidine alkaloids (RF-00000230-TOX)
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Additional substance description:
Curassavine
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Analytical method code:
GC-MS (F046A)
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Yes/No Qualitative:
Positive/Present (POS)
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Result type:
Qualitative Value (Binary) (BIN)
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Internal remarks:
curassavine (pyrrolizidine alkaloid)
Composition #3: Romussi, G., Falsone, G., Wendisch, D., Parodi, B. Inhaltsstoffe von Boraginaceae, 7. Anchusosid‐8 und ‐9: Zwei neue Triterpensaponine aus Anchusa officinalis L.. liebigs annalen der chemie, 1984, vol. 1984, no. 11, p. 1869–1872. DOI: 10.1002/jlac.198419841113.
[
DOI link]
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Plant part:
Aerial part of plants (as part-nature) (A166F)
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Extraction/Preparation method:
Solvent extraction (A0BZR)
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Additional extraction description:
Ethanol
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Substance:
pentacyclic triterpene saponins (RF-00004334-PAR)
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Additional substance description:
Anchuchoside 8 and 9
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Analytical method code:
Standard Chromatographic tests (paper- thin layer- and column chromatography) (F016A)
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Analytical method - additional description:
EI-MS; 'H and C NMR spectroscopy
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Yes/No Qualitative:
Positive/Present (POS)
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Result type:
Qualitative Value (Binary) (BIN)
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Internal remarks:
Anchusoside 8 and 9 ( pentacyclic triterpene saponins )
Composition #4: BROCHDUE, AI., AASEN, AJ. ALKALOIDS OF ANCHUSA-OFFICINALIS L IDENTIFICATION OF THE PYRROLIZIDINE ALKALOID LYCOPSAMINE . acta chemica scandinavica series b-organic chemistry and biochemistry, 1980, vol. 34, no. 1, p. 75–77. DOI: 10.3891/acta.chem.scand.34b-0075.
[
DOI link]
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Plant part:
Seed (as part-nature) (A066P)
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Extraction/Preparation method:
Solvent extraction (A0BZR)
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Additional extraction description:
methanol in a Soxhlet extractor
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Substance:
Laburnine (RF-00000288-TOX)
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Additional substance description:
Laburnine and derivatives
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Analytical method code:
GC-MS (Q) (F344A)
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Yes/No Qualitative:
Positive/Present (POS)
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Result type:
Qualitative Value (Binary) (BIN)
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Internal remarks:
Laburnine and derivatives (seeds)
Composition #5: BROCHDUE, AI., AASEN, AJ. ALKALOIDS OF ANCHUSA-OFFICINALIS L IDENTIFICATION OF THE PYRROLIZIDINE ALKALOID LYCOPSAMINE . acta chemica scandinavica series b-organic chemistry and biochemistry, 1980, vol. 34, no. 1, p. 75–77. DOI: 10.3891/acta.chem.scand.34b-0075.
[
DOI link]
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Plant part:
Roots and other underground parts (as part-nature) (A067M)
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Extraction/Preparation method:
Solvent extraction (A0BZR)
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Additional extraction description:
methanol in a Soxhlet extractor
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Substance:
Lycopsamine (RF-00000228-TOX)
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Additional substance description:
Lycopsamine and derivatives
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Analytical method code:
Standard Chromatographic tests (paper- thin layer- and column chromatography) (F016A)
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Analytical method - additional description:
‘H-NMR
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Yes/No Qualitative:
Positive/Present (POS)
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Result type:
Qualitative Value (Binary) (BIN)
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Internal remarks:
Lycopsamine and derivatives (roots and green parts)